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- Synthesis, Characterization, and Spectroscopic Properties of ZnO Nanoparticles
- SYNTHESIS AND CHARACTERIZATION OF ZnO NANO-PARTICLES
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Synthesis, Characterization, and Spectroscopic Properties of ZnO Nanoparticles
These metrics are regularly updated to reflect usage leading up to the last few days. Citations are the number of other articles citing this article, calculated by Crossref and updated daily. Find more information about Crossref citation counts.
The Altmetric Attention Score is a quantitative measure of the attention that a research article has received online. Clicking on the donut icon will load a page at altmetric. Find more information on the Altmetric Attention Score and how the score is calculated. The potential ecotoxicity of nanosized zinc oxide ZnO , synthesized by the polyol process, was investigated using common Anabaena flos-aquae cyanobacteria and Euglena gracilis euglenoid microalgae. The photosynthetic activities of these microorganisms, after addition of ZnO nanoparticles, varied with the presence of protective agents such as tri- n -octylphosphine oxide TOPO and polyoxyethylene stearyl ether Brij used to control particle size and shape during the synthesis.
In the case of Anabaena flos-aquae , the photosynthetic activity, after addition of ZnO, ZnO-TOPO, and ZnO-Brij, decreased progressively due to stress induced by the presence of the nanoparticles in the culture medium. On the other hand, after 10 days, a progressive increase of the photosynthetic activity was observed after contact with ZnO and ZnO-Brij nanoparticles. In the case of Euglena gracilis , cell death was observed after contact with all nanoparticles.
Transmission electron microscopy TEM analyses of ultrathin sections of microorganisms showed that polysaccharides produced by Anabaena flos-aquae avoid particle internalization after contact with ZnO and ZnO-Brij nanoparticles. On the other hand, nanoparticle internalization was observed after contact with all nanoparticles in the presence of Euglena gracilis and also with ZnO-TOPO nanoparticles after contact with Anabaena flos-aquae.
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SYNTHESIS AND CHARACTERIZATION OF ZnO NANO-PARTICLES
Government Kalasala, Jangareddygudem , India. ZnO nanoparticles have been synthesized by precipitation method from Zinc nitrate. The powder was characterized by X-ray diffraction, scanning electron microscopy, transmission electron microscopy, selected-area electron diffraction, UV-vis optical absorption, and photoluminescence spectroscopy analyses. XRD patterns showed that ZnO nanoparticles have hexagonal unit cell structure. The synthesis method has potential for application in manufacturing units due to ease processing and more economical reagents. Nowadays, there has been an increasing demand for the development of nanosized semiconductors due to their significant electrical and optical properties which are highly useful in fabricating nanoscaled optoelectronic and electronic devices with multifunctionality [ 1 — 3 ]. Among various semiconducting materials, zinc oxide ZnO is a distinctive electronic and photonic wurtzite n-type semiconductor with a wide direct band gap of 3.
Narrow band gap zinc oxide (ZnO) nanoparticles (NPs) were synthesized using unboiled and boiled leaf extracts of Costus woodsonii. The as-.
Zinc oxide nanoparticles were synthesized using a simple precipitation method with zinc sulfate and sodium hydroxide as starting materials. The synthesized sample was calcined at different temperatures for 2 h. SEM images show various morphological changes of ZnO obtained by the above method. The average crystallite sizes of the samples were calculated from the full width at half maximum of XRD peaks by using Debye-Scherrer's formula and were found to be in the nanorange. EDS shows that the above route produced highly pure ZnO nanostructures.
Cynara scolymus leaves were used in the green synthesis of zinc oxide nanoparticles ZnO NPs. ZnO NPs was confirmed by the formation of a white precipitate. The use of SEM confirmed the spherical shape of the nanoparticles, which had an average size of The nanoparticle zinc X-ray power diffraction XRD spectra confirmed the crystalline nature of the nanoparticles.
In this work, nanoparticles of zinc oxide ZnO-NPs were synthesized using acetic acid, ethanol and ethylene glycol as solvents. To determine the physicochemical and structural characteristics of the synthesized nanoparticles, IR spectroscopy, X-ray diffraction, UV—Vis spectroscopy and transmission electron microscopy were used. The band gap of ZnO-Nps depends of synthesis solvent used: 3. Based on the information from the characterization of the ZnO-NPs synthesized, the spheroidal nanoparticles were selected, to determine their antifungal capacity on cultures of Aspergillus niger strains. This is a preview of subscription content, access via your institution.